Trifluoroacetic acid → HCID 22623919, compound

Participants

Reaction Steps

A mixture of 2-tert-butyloxy-5-chloro-8-nitro-6-(pyrrolidin-1-yl)-benzo[de]isoquinoline-1,3-dione (0.2 g, 0.47 mmol, from Example M3-A) and TFA (1.6 mL) was stirred at room temperature for 2 hours and poured into ice water. The solid was collected, washed with water and ether, and dried to give 0.12 g of the title compound, mp 209-210° C.

Provenance & Evidence