反应详情

3-Bromoindan-1-one (1.5) was dissolved in diethyl ether (10 ml). The temperature was kept at +2-+4 while TEA (2.7 ml) was added. The resulting mixture was further stirred at +2-+4 for 2 hours. The precipitated salt was filtered off and the filtrate evaporated. The crude inden-1-one was used for further reaction without purification. Yield was 0.9 g.

1. additionwas added
2. filtrationThe precipitated salt was filtered off
3. customthe filtrate evaporated
4. customThe crude inden-1-one was used for further reaction without purification