HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → alpha-p-cyclohexylphenyl-N-p-chlorophenylnitrone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Chlorophenylhydroxylamine | HCID 69983 | — |
| Reactant | p-Cyclohexylbenzaldehyde | HCID 119689 | — |
| Product | alpha-p-cyclohexylphenyl-N-p-chlorophenylnitrone | HCID 86736527 | — |
Reaction Steps
p-Chlorophenylhydroxylamine (0.05 moles) was dissolved in warm 95% ethanol (40 cc) and was treated with p-cyclohexylbenzaldehyde (0.05 moles) with vigorous stirring. The solid which formed was collected, washed with 95% ethanol, and was recrystallized from ethanol to give α-p-cyclohexylphenyl-N-p-chlorophenylnitrone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04224340 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-a08ba00d67694fe28cd804ece3bd15f7 |
| Source note | uspto-grants-1980_09 |