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HRID27919

反应详情

EQUATION

反应方程式

HRID 27919 的结构方程式

REACTANTS

反应物

2
结构：ONc1ccccc1
HCID7518

N-Phenylhydroxylamine

C6H7NO

结构：Cc1cc(Cl)ccc1N=Cc1ccc(Cl)cc1
HCID13017552

未命名化合物

PRODUCTS

生成物

1
结构：[O-][N+](=Cc1ccc(Cl)cc1)c1ccccc1
HCID254504

Benzenamine, N-[(4-chlorophenyl)methylene]-, N-oxide, [N(E)]-

C13H10ClNO

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

2 次

PROCEDURE

实验过程

N-phenylhydroxylamine (0.052 mole) was dissolved in ether (20 cc). This solution was treated with N-(p-chlorobenzylidene)-2-methyl-4-chloroaniline (13.8 g.) dissolved in ether (50 cc). After 15 min., white crystals had begun to form. Filtration and washing with ether gave α-p-chlorophenyl-N-phenylnitrone.

WORKUP

后处理

  1. customto form
  2. filtrationFiltration
  3. washwashing with ether