Sodium Sulfate → HCID 15541828, compound

Participants

Reaction Steps

To a suspension of 33 mg (0.87 mmol) of lithium aluminum hydride in 0.5 ml of diethyl ether, 100 mg (0.29 mmol) of the material prepared in Example 14 in 0.5 ml of diethyl ether and 0.5 ml of THF. The mixture was stirred for 3 h. Na2SO4 10H2O was added, and the mixture stirred for 30 min at ambient temperature. The solid was filtered and the organic solution was concentrated in vacuo. Precipitation with diethyl ether afforded 65 mg (64%) of the title compound. Analysis calculated for C19H30N2O2S 0.75H2O: %C, 62.69; %H, 8.72; %N, 7.69. Found: %C, 62.73; %H, 7.96; %N, 7.32. Field Desorption Mass Spectrum: M=350.

Provenance & Evidence