Thionyl Chloride → 9-gamma-Chloropropyl-9,10-dihydro-9,10-methanoanthracene

HRID 27953Notes

Reaction equation

HRID 27953 reaction equation
O[CH2:2][CH2:3][CH2:4][C:5]12[CH2:19][CH:12]([C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=31)[C:11]1[C:6]2=[CH:7][CH:8]=[CH:9][CH:10]=1.S(Cl)([Cl:22])=O>C1C=CC=CC=1>[Cl:22][CH2:2][CH2:3][CH2:4][C:5]12[CH2:19][CH:12]([C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=31)[C:11]1[C:6]2=[CH:7][CH:8]=[CH:9][CH:10]=1

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 20519949HCID 20519949, compound

Product 1

HCID 205199629-gamma-Chloropropyl-9,10-dihydro-9,10-methanoanthracene

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The starting 9-γ-chloropropyl-9,10-dihydro-9,10-methanoanthracene was prepared by reacting 9-γ-hydroxypropyl-9,10-dihydro-9,10-methanoanthracene with thionyl chloride in benzene.

Sources & evidence

ORD record
ord-95fa816975564eb4bb595bd5fabf49c6
Source dataset
uspto-grants-1980_09
Patent number
US04224344

Reaction notes

Loading…