Ethyl alpha-oxobenzenebutanoate → HCID 23322755, compound

HRID 279839Notes

Reaction equation

HRID 279839 reaction equation
[CH2:1]([O:3][C:4]([CH:6]([N:8]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH:10]([NH2:17])[C:9]1=[O:18])[CH3:7])=[O:5])[CH3:2].O=[C:20]([CH2:26][CH2:27][C:28]1[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=1)[C:21]([O:23][CH2:24][CH3:25])=[O:22]>C(O)C>[CH2:1]([O:3][C:4]([CH:6]([N:8]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH:10]([NH:17][CH:20]([C:21]([O:23][CH2:24][CH3:25])=[O:22])[CH2:26][CH2:27][C:28]2[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=2)[C:9]1=[O:18])[CH3:7])=[O:5])[CH3:2]

Participants

4

Reactant 2

HCID 562087Ethyl alpha-oxobenzenebutanoateHCID 23322734HCID 23322734, compound

Product 1

HCID 23322755HCID 23322755, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Hydrogenate 2.42 g 1-(1-ethoxycarbonylethyl)-3-aminoperhydroazonin-2-one and 3.09 g ethyl 2-oxo-4-phenylbutyrate in 100 ml ethanol containing 0.60 g acetic acid as described in Example 1.

Sources & evidence

ORD record
ord-b4fed226285243e79752bf7844d0da44
Source dataset
uspto-grants-1986_05
Patent number
US04587238

Reaction notes

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