Thionyl Chloride → HCID 70456472, compound

HRID 279844Notes

Reaction equation

HRID 279844 reaction equation
[C:1]([O:4][N:5]1[CH:9]=[C:8]([CH2:10]O)[N:7]=[C:6]1[CH2:12][CH:13]=[CH2:14])(=[O:3])[CH3:2].S(Cl)([Cl:17])=O>C(Cl)Cl>[ClH:17].[C:1]([O:4][N:5]1[CH:9]=[C:8]([CH2:10][Cl:17])[N:7]=[C:6]1[CH2:12][CH:13]=[CH2:14])(=[O:3])[CH3:2]

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 54454960HCID 54454960, compound

Product 1

HCID 70456472HCID 70456472, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

React allyl-4-hydroxymethylimidazol-1-yl acetate with excess thionyl chloride in CH2Cl2 at ice bath temperatures for about 8 hours to form the title compounds.

Sources & evidence

ORD record
ord-8b5300fbb82c41ba98e80bfb001d40b2
Source dataset
uspto-grants-1986_05
Patent number
US04587241

Reaction notes

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