HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cornforth reagent → HCID 70466070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cornforth reagent | HCID 2724130 | — |
| Reactant | HCID 70466692 | HCID 70466692 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 70466070 | HCID 70466070 | 100.6% |
Reaction Steps
5.0 g of 2-chloro-3,3-ethylenedioxy-5α-androst-1-en-17β-ol is stirred in 50 ml of dimethylformamide with 10 g of pyridinium dichromate for 17 hours at room temperature and then worked up as described in Example 10B. After evaporation, 5 g of 2-chloro-3,3-ethylenedioxy-5α-androst-1-en-17-one is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04587235 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-5a8f44faddf241fc8e4769e2641a9c57 |
| Source note | uspto-grants-1986_05 |