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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 279886Generated: October 26, 2026

Methyl carbazate → N-(methoxycarbonyl)-N'-(2-benzylcyclohexylidene)-hydrazine

https://huagongshe.com/reaction/279886

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl carbazateHCID 80519—
Reactant2-Benzylcyclohexan-1-oneHCID 98945—
SolventEthanolHCID 702—
ProductN-(methoxycarbonyl)-N'-(2-benzylcyclohexylidene)-hydrazineHCID 5710641596.9%

Reaction Steps

18.83 g (0.1 mole) of 2-benzylcyclohexan-1-one and 9.0 g (0.1 mole) of N-methoxycarbonyl hydrazine are dissolved in 100 cm3 of anhydrous ethanol, and the solution is boiled for 2 hours. Then it is cooled, and the separated crystals are filtered off. 18.2 g (96.9%) of the named compound are obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04587261
Source datasetuspto-grants-1986_05
ORD IDord-22f0f84b0feb478f8e647024c2ae3d75
Source noteuspto-grants-1986_05