HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylhomoveratrylamine → HCID 13645635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylhomoveratrylamine | HCID 77039 | — |
| Reactant | HCID 13645634 | HCID 13645634 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13645635 | HCID 13645635 | — |
Reaction Steps
N-isopropyl-N-(3-oxopropyl)-2,3,4-trimethoxybenzenesulfonamide prepared in the previous paragraph (7.50 g, 0.0384 m), N-methyl-homoveratrylamine (6.83 g, 0.350 m) in absolute ethanol (100 ml) containing PtO2 (0.5 g) was shaken under hydrogen all day. The crude product (8.01 g) obtained from this procedure after chromatography gave the pure title compound, a white gum (5.71 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04587360 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-b0522054fcb948e2a372f6d7df5853e2 |
| Source note | uspto-grants-1986_05 |