HRID280223

反应详情

EQUATION

反应方程式

HRID 280223 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

5-[p-(Hydroxymethyl)phenethyl]imidazo[1,5-a]pyridine (2.52 g) is refluxed in 100 ml of methylene chloride with 25.2 g of activated manganese dioxide for 24 hours. The mixture is filtered and evaporated to yield 5-(p-formylphenethyl)imidazo[1,5-a]pyridine.

WORKUP

后处理

  1. filtrationThe mixture is filtered
  2. customevaporated