HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylaniline → HCID 13588334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 13588349 | HCID 13588349 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 13588334 | HCID 13588334 | — |
Reaction Steps
A solution of 10.2 g of the above carboxylic acid in 135 ml of chloroform containing 0.4 ml of N,N-dimethylaniline and 20.0 ml of phosphorus oxychloride was heated at reflux for three hours, cooled, and reddish-orange crystals of the title compound, mp 239-241° C., were collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588730 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-970029655be047a88908080b7db7f84f |
| Source note | uspto-grants-1986_05 |