HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylaniline → HCID 13588338, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylaniline | HCID 949 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 13588353 | HCID 13588353 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 13588338 | HCID 13588338 | — |
Reaction Steps
A mixture of 9.7 g of 2-chloro-3,5-dinitro-6-[[4-(phenylmethoxy)phenyl]amino]benzoic acid, 200 ml of 1,2-dichloroethane, 20 ml of phosphorus oxychloride, and 1.0 ml of N,N-dimethylaniline was heated under reflux for 30 minutes. Upon cooling, a solid formed which was collected and washed with 1,2-dichloroethane providing the title compound, mp 217°-220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588730 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-0219104bf1e6464f8fca80f2f9b0ea9d |
| Source note | uspto-grants-1986_05 |