HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13135477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 13135443 | HCID 13135443 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13135477 | HCID 13135477 | 99.1% |
Reaction Steps
NaBH4 (0.6 g) was added portionwise to a solution of 2-methyl-3-(1-imidazolyl)-2,3-dihydro-4H-1-benzopyran-4 one (1.3 g) in MeOH (70 ml) at room temperature. The mixture, stirred for 2 hours, added with water (300 ml), extracted with CHCl3, dried and evaporated to dryness gave 2-methyl-3-(1-imidazolyl)-2.3-dihydro-4H-1-benzopyran-4-ol (1.3 g);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588738 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-ad317fabb95d46d2a6a53d49d535d375 |
| Source note | uspto-grants-1986_05 |