HCID 12769232, compound → 3-Azido-4-(2-hydroxyethyl)-2-azetidinone

HRID 28031Notes

Reaction equation

HRID 28031 reaction equation
C1(CC(NC2C(=O)N3C2CCOC3(C)C)=O)C=CC=CC=1.[N:22]([CH:25]1[C:32](=[O:33])[N:31]2[CH:26]1[CH2:27][CH2:28][O:29]C2(C)C)=[N+:23]=[N-:24]>>[N:22]([CH:25]1[CH:26]([CH2:27][CH2:28][OH:29])[NH:31][C:32]1=[O:33])=[N+:23]=[N-:24]

Participants

3

Procedure

Following the procedure of Example 7 except substituting for the indicated 7-phenylacetamido-8-oxo-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane the 7-azido-8-oxo-2,2-dimethyl-3-oxa-1-azabicyclo[4.2.0]octane, the title compound is obtained.

Sources & evidence

ORD record
ord-ae96b4ec10ed4cfeb9514307ae02b2f3
Source dataset
uspto-grants-1980_09
Patent number
US04224336

Reaction notes

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