HRID280313

反应详情

EQUATION

反应方程式

HRID 280313 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in the manner described in Example 9 using phenylglyoxal and 3-(4-Methylphenyl)propanamine. Recrystallization of the chromatographed material from benzene-hexane gave the title compound m.p. 114-116. τ(CDCL3) 8.15 (2H, m), 7.7 (3H, s), 6.9-7.5 (6H, m+2H, disappears with D2O), 5.3 (1H, m), 2.9 (4H, s), 2.7 (5H, m).

WORKUP

后处理

  1. customThe title compound was prepared in the manner
  2. customRecrystallization of the chromatographed material from benzene-hexane