HRID280316

反应详情

EQUATION

反应方程式

HRID 280316 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in the manner described in Example 9 using 3-chlorophenylglyoxal and 3-(4-methylphenyl)-1,1-dimethylpropanamine. The chromatographed material was recrystallized from cyclohexane to give the title compound m.p. 136. τ(CDCL3 +d6DMSO) 8.9 (6H, s), 8.2-8.4 (2H, m), 7.7 (3H, s), 7.0-7.6 (4H, m), 5.35 (1H, dd), 2.9 (4H, s), 2.5-2.7 (5H, m).

WORKUP

后处理

  1. customThe title compound was prepared in the manner
  2. customThe chromatographed material was recrystallized from cyclohexane