HRID280317

反应详情

EQUATION

反应方程式

HRID 280317 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in the manner described in Example 3 using 2-hydroxy-2-phenylethanamine and (4-methylphenoxy)propan-2-one. Recrystallization from heptane gave the title compound m.p. 87-105. τ(CDCL3) 8.9 (3H, d, J=6 Hz), 7.7 (3H, s), 6.7-7.5 (3H, +2H (disappears with D2O)), 6.2 (2H, m), 5.3 (1H, m), 3.3 (2H, d, J=9 Hz), 2.9 (2H, d, J=9 Hz), 2.7 (5H, m).

WORKUP

后处理

  1. customThe title compound was prepared in the manner
  2. customRecrystallization from heptane