HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 53826873, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | N,O-Dimethylhydroxylamine | HCID 14232 | — |
| Reactant | 5-[4-Isocyanato-2-(trifluoromethyl)phenoxy]-1,2-benzothiazole | HCID 23320449 | — |
| Product | HCID 53826873 | HCID 53826873 | 83% |
Reaction Steps
A solution of 6.1 parts of N-methoxy-N-methylamine in 100 parts of diethyl ether was added to a solution of 33.6 parts of 5-(4'-isocyanato-2'-trifluoromethylphenoxy)-benzisothiazole in 300 parts of diethyl ether at from 20 to 30° C., the reaction mixture was stirred for 12 hours at this temperature and the resulting precipitate was then isolated. 33 parts (83% of theory) of 5-[4'-(N-methoxy-N-methylaminocarbonylamino)-2'-trifluoromethylphenoxy]-benzisothiazole of melting point 197° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04589910 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-cf6cc3cdd3604b96a91873c33f610a65 |
| Source note | uspto-grants-1986_05 |