HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → N,N,N,2,2-Pentamethylpropan-1-aminium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Tributylamine | HCID 7622 | — |
| Reactant | Neopentylamine | HCID 79882 | — |
| Product | N,N,N,2,2-Pentamethylpropan-1-aminium iodide | HCID 13652289 | — |
Reaction Steps
11.51 Grams of neopentylamine (Aldrich), 48.7 grams of tributyl amine and 100 ml of DMF were mixed and cooled. 56 Grams of methyl iodide (Aldrich) were added dropwise and the reaction was carried out and worked up as in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04589977 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-c51cb8b2898444f0a0cd172d02f82682 |
| Source note | uspto-grants-1986_05 |