HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → 1-(2',6'-Diethylphenyl)-4-dimethylaminomethylene amino-1,2-dihydro-1,3,5-triazin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 1-(2',6'-Diethylphenyl)-4-amino-1,2-dihydro-1,3,5-triazin-2-one | HCID 13039376 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-(2',6'-Diethylphenyl)-4-dimethylaminomethylene amino-1,2-dihydro-1,3,5-triazin-2-one | HCID 53741429 | — |
Reaction Steps
1-(2',6'-diethylphenyl)-4-amino-1,2-dihydro-1,3,5-triazin-2-one (5.9 g, 20 mmo) is combined with 30 ml of CH3CN, none of the solid dissolves. To this is added 1.19 g (10 mmol) of N,N-dimethylformamide dimethylacetal. The solid dissolves within seconds. The reaction solution was stirred overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04225315 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-ea9808665c6c43fdac34f3d842e7e774 |
| Source note | uspto-grants-1980_09 |