Ethanol → HCID 13649663, compound

Participants

Reaction Steps

A mixture of 4-(2,6-dichlorobenzyl)benzyl bromide (7.49 g, 21.8 mmol) and sodium azide (4.19 g, 64.5 mmol) in absolute ethanol (100 ml) was refluxed 5 hours, cooled, and evaporated under vacuum. The residue was triturated wit diethyl ether (100 ml), filtered, and evaporated under vacuum to provide 6.5 g (98%) 4-(2,6-dichlorobenzoyl)benzyl azide, m.p. 92°-94° C.

Provenance & Evidence