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HRID280989

反应详情

EQUATION

反应方程式

HRID 280989 的结构方程式

REACTANTS

反应物

1
结构：ClCc1ccccc1
HCID7503

Benzyl chloride

C7H7Cl

PRODUCTS

生成物

1
结构：Cc1cccc(Cc2ccccc2)c1Cc1ccccc1
HCID3034397

1,1'-[(3-Methyl-1,2-phenylene)bis(methylene)]dibenzene

C21H20

收率 61.3%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

To a reaction vessel were added 2500 g of toluene and 50 g of FeCl3 and reaction was carried out for 3 hours by adding 1500 g of benzyl chloride with stirring at room temperature. After the reaction, the catalyst was deactivated and 660 g of dibenzyltoluene was obtained.

WORKUP

后处理

  1. additionTo a reaction vessel were added
  2. customAfter the reaction