HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetophenone → 2-Amino-4-phenylthiazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetophenone | HCID 7410 | — |
| Edukt | Sulfuryl chloride | HCID 24648 | — |
| Edukt | Thiourea | HCID 2723790 | — |
| Produkt | 2-Amino-4-phenylthiazole | HCID 40302 | — |
Reaktionsschritte
Carefully mix 360 g (3 mols) of acetophenone and 455 g (6 mols) of thiourea; then add 264 ml (3.3 mols) of sulfuryl chloride in small fractions. The reaction is exothermic and the sulfuryl chloride is added over the course of two hours.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04225610 |
| Quelldatensatz | uspto-grants-1980_09 |
| ORD ID | ord-2aea7c5200de4436ba673fde5ea56baa |
| Quellennotiz | uspto-grants-1980_09 |