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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 28237Generated: October 28, 2026

Hydroxyamine hydrochloride → HCID 13051039, compound

https://huagongshe.com/reaction/28237

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantSodium FormateHCID 2723810—
Reactant9-hydroxy-1-oxo-1H-naphtho[2,1-b]pyran-2-carboxaldehyde acetateHCID 86737239—
SolventFormic AcidHCID 284—
ProductHCID 13051039HCID 13051039—

Reaction Steps

A mixture of compound 5, hydroxylamine hydrochloride and sodium formate is refluxed in formic acid to provide 9-hydroxy-1-oxo-1H-naphtho[2,1-b]pyran-2-carbonitrile, Compound 8.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04225722
Source datasetuspto-grants-1980_09
ORD IDord-a6c9b2547c6345418a3d85395c0a5041
Source noteuspto-grants-1980_09