HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 12363926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Benzyloxy-3-(methanesulfonylamino)phenyl acetate | HCID 54103892 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 12363926 | HCID 12363926 | — |
Reaction Steps
A mixture of 7.7 g (0.023 mol) of 4-benzyloxy-3-(N-methylsulphonylamino)phenyl acetate, 4.75 g (0.035 mol) of crushed potassium carbonate and 3.3 ml (0.0276 mol) of benzyl bromide in 150 ml of anhydrous acetone is stirred at reflux temperature for 4 hours. After filtration and evaporation, the compound of the title is obtained, which is recrystallized in ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07419974B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-306383420c824b989835112af802b182 |
| Source note | uspto-grants-2008_09 |