HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 3-Chloro-4-(2-trimethylsilylethoxymethoxy)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 3-Chloro-4-hydroxybenzaldehyde | HCID 17022 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 2-Chloromethyl 2-(trimethylsilyl)ethyl ether | HCID 2724271 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-Chloro-4-(2-trimethylsilylethoxymethoxy)benzaldehyde | HCID 86591405 | — |
Reaction Steps
5 g (31.93 mmol) of 5-chloro-4-hydroxybenzaldehyde are dissolved in 300 ml of methylene chloride and 6.7 ml (38.3 mmol) of N,N-diisopropyl-N-ethylamine and 5.9 ml (33.52 mmol) of 2-trimethylsilylethoxymethyl chloride (SEMCl) are added to this at 0° C. The mixture is allowed to return to room temperature and stirred overnight. Water is then added and the mixture is extracted with methylene chloride. The organic phase is dried and the solvent is evaporated off. The product of the title is obtained, which is purified by chromatography on a silica gel column, eluting with a 95/5 and then 9/1 heptane/ethyl acetate mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07419974B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-df80d05eca0843ef96b1d0374c0d5837 |
| Source note | uspto-grants-2008_09 |