HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-Chloro-2-methoxy-benzylideneamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 5-Chloro-2-methoxy-benzimidic acid ethyl ester | HCID 66851468 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5-Chloro-2-methoxy-benzylideneamine | HCID 86004319 | 129% |
Reaction Steps
A mixture of 5-chloro-2-methoxy-benzimidic acid ethyl ester (1.0 g, 4.0 mmol) and a solution of ammonia in methanol (7.0 M, 50 ml) was stirred for 48 hours. Evaporation of volatiles under reduced pressure provided 5-chloro-2-methoxy-benzylideneamine (0.875 g, 99% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07419984B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-e156bd4fee62435594200402a7c630ce |
| Source note | uspto-grants-2008_09 |