HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethyl borate → 5-Bromo-2-chlorophenylboronic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethyl borate | HCID 8470 | — |
| Reactant | 4-Bromo-1-chloro-2-iodobenzene | HCID 51000071 | — |
| Reactant | HCID 178418918 | HCID 178418918 | — |
| Product | 5-Bromo-2-chlorophenylboronic acid | HCID 46736816 | 36% |
Reaction Steps
Following the method described in Example 81, 4-bromo-1-chloro-2-iodo-benzene, isopropylmagnesium chloride and trimethylborate provided 5-bromo-2-chloro-phenylboronic acid (36% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07419984B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-880846cffbb445df8bfdbdfb9feb21c8 |
| Source note | uspto-grants-2008_09 |