HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Z)-3-(3-nitro-4-chlorophenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile → (E)-3-(3-nitro-4-chlorophenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Z)-3-(3-nitro-4-chlorophenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile | HCID 10714483 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | (E)-3-(3-nitro-4-chlorophenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile | HCID 10619446 | 26.7% |
Reaction Steps
1.5 g of (Z)-3-(3-nitro-4-chlorophenyl)-2-(3,4,5-trimethoxyphenyl)-prop-2-ene-nitrile was dissolved in 500 ml of acetone and the solution was reacted in a photochemical apparatus (visible light) for 1 hour. The reaction mixture was concentrated and a half of it was purified on a silica gel plate to give 400 mg of the intended compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731353 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-0713a93170224a6cbc1dbbb08f705236 |
| Source note | uspto-grants-1998_03 |