HRID29371

反应详情

EQUATION

反应方程式

HRID 29371 的结构方程式

PROCEDURE

实验过程

To 174 mg of 4-furan-3-yl-3-methyl-benzofuran-2-carboxylic acid tert-butyl ester was added 4 mL of TFA/dichloromethane (1:1). The solution was stirred at room temperature for 2 h. The solvents were removed under vacuum and the residue was triturated with ether. Filtration gave 124 mg of of 4-furan-3-yl-3-methyl-benzofuran-2-carboxylic acid as a white solid.

WORKUP

后处理

  1. customThe solvents were removed under vacuum
  2. customthe residue was triturated with ether
  3. filtrationFiltration