HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzohydrazide → 4-Fluoro-benzoic acid-(1-imino-ethyl)-hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzohydrazide | HCID 9972 | — |
| Reactant | Ethanimidic acid, ethyl ester, hydrochloride (1:1) | HCID 2724290 | — |
| Product | 4-Fluoro-benzoic acid-(1-imino-ethyl)-hydrazide | HCID 68492563 | — |
Reaction Steps
Prepared from 7.2 g (58 mmol) ethyl acetimidate hydrochloride and 5.00 g (32 mmol) 4-fluoro-benzoic acid hydrazide analogously to the method described for intermediate product la). Yield: 5.78 g (91%); mass spectroscopy [M+H]+=196.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423036B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-b41695718a664a768a837ad4a3875418 |
| Source note | uspto-grants-2008_09 |