HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetate → HCID 11596699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetate | HCID 84468 | — |
| Reactant | 1-(2,3,5,6-Tetramethyl-benzyl)-cyclopropylamine | HCID 23106145 | — |
| Reactant | 5-(benzyloxy)-8-(dihydroxyacetyl)-2H-1,4-benzoxazin-3(4H)-one | HCID 23106148 | — |
| Product | HCID 11596699 | HCID 11596699 | — |
Reaction Steps
Prepared according to general method 3 from 329 mg (1 mmol) 5-benzyloxy-8-(2,2-dihydroxy-acetyl)-4H-benzo[1,4]oxazin-3-one and 203 mg (1 mmol) 1-(2,3,5,6-tetramethyl-benzyl)-cyclopropylamine. Yield: 93 mg (18%, trifluoroacetate); mass spectroscopy: [M+H]+=411.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423035B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-45a780a222ac46b99abb9860b2d90de6 |
| Source note | uspto-grants-2008_09 |