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HRID29888

反应详情

EQUATION

反应方程式

HRID 29888 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)CC(=O)c1ccccc1
HCID7170

Ethyl benzoylacetate

C11H12O3

结构：Cl.N=C(N)c1ccc(Cl)cc1
HCID203436

Benzamide, p-chloro-, hydrochloride (7CI)

C7H8Cl2N2

PRODUCTS

生成物

1
结构：Oc1cc(-c2ccccc2)nc(-c2ccc(Cl)cc2)n1
HCID178515558

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 3-oxo-3-phenyl-propionic acid ethyl ester and 4-chloro-benzamidine hydrochloride according to general procedure 1. 1H NMR (DMSO-d6, 400 MHz) δ 6.97 (s, 1H), 7.50-7.58 (m, 3H), 7.16 (d, J=8.5 Hz, 2H), 8.10-8.20 (m, 2 H), 8.30 (d, J=8.5 Hz, 2H), 12.50 (br s, 1H); MS: m/z (ESI) 283 (M+H).