huagongshe.com
HRID29893

反应详情

EQUATION

反应方程式

HRID 29893 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)CC(=O)C(C)C
HCID81583

Ethyl isobutyrylacetate

C8H14O3

结构：Cl.N=C(N)c1cc(Cl)cc(Cl)c1
HCID2743159

3,5-Dichlorobenzene-1-carboximidamide--hydrogen chloride (1/1)

C7H7Cl3N2

PRODUCTS

生成物

1
结构：CC(C)c1cc(O)nc(-c2cc(Cl)cc(Cl)c2)n1
HCID178439458

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-methyl-3-oxo-pentanoic acid ethyl ester and 3,5-dichloro-benzamidine hydrochloride according to general procedure 1. 1H NMR (DMSO-d6, 400 MHz) δ 1.20-1.26 (m, 6H), 2.80-2.90 (m, 1H), 6.34 (s, 1H), 7.82(s, 1H), 8.18 (s, 2H), 12.50 (br s,1H); MS: m/z (ESI) 283 (M+H).