huagongshe.com
HRID29896

反应详情

EQUATION

反应方程式

HRID 29896 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)C1CN(Cc2ccccc2)CCC1=O
HCID102624

1-Benzyl-3-ethoxycarbonyl-4-piperidone

C15H19NO3

结构：Cl.N=C(N)c1cccc([N+](=O)[O-])c1
HCID12456162

3-Nitrobenzene-1-carboximidamide--hydrogen chloride (1/1)

C7H8ClN3O2

PRODUCTS

生成物

1
结构：O=[N+]([O-])c1cccc(-c2nc(O)c3c(n2)CCN(Cc2ccccc2)C3)c1
HCID178526607

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 1-benzyl-4-oxo-piperidine-3-carboxylic acid ethyl ester and 3-nitro-benzamidine hydrochloride according to general procedure 1. 1H NMR (DMSO-d6, 400 MHz) δ 2.76 (s, 4H), 3.28 (s, 2H), 3.71 (s, 2H), 7.25-7.40 (m, 6H), 7.81 (t, J=8.0 Hz, 1H), 8.35-8.40 (m, 1H), 8.52 (d, J=8.0 Hz, 2H), 8.93 (s, 1H); MS: m/z (ESI) 363 (M+H).