HRID29912

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID123062

1-(Bromomethyl)-4-(trifluoromethyl)benzene

C8H6BrF3

结构：CC(C)c1cc(O)nc(-c2cccc([N+](=O)[O-])c2)n1

HCID178439455

未命名化合物

2 次

PRODUCTS

生成物

结构：CC(C)c1cc(OCc2ccc(C(F)(F)F)cc2)nc(-c2cccc([N+](=O)[O-])c2)n1

HCID10070573

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 6-isopropyl-2-(3-nitro-phenyl)-pyrimidin-4-ol (which was obtained in Intermediate 8) and 4-(trifluoromethyl)benzyl bromide according to Method A; 1H NMR (DMSO-d6, 300 MHz) δ 1.30 (d, J=6.8 Hz, 6H), 3.00-3.10 (m, 1H), 5.69 (s, 2H), 6.95 (s, 1H), 7.75-7.85 (m, 4H), 7.84 (t, J=8.1 Hz, 1H), 8.38 (t, J=8.1 Hz, 1H), 8.80 (d, J=7.8 Hz, 1H), 9.08 (s, 1H); LC retention 4.18 min; MS: m/z (ESI) 418 (M+H).

WORKUP

后处理

customLC retention 4.18 min