2-Bromo-5-methoxybenzoic acid → HCID 69213029, compound

HRID 30023Notes

Reaction equation

HRID 30023 reaction equation
Br[C:2]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].C([Li])CCC.[CH3:18][O:19][C:20]1[CH:31]=[C:30]([O:32][CH3:33])[CH:29]=[CH:28][C:21]=1[C:22](N(OC)C)=[O:23]>>[CH3:18][O:19][C:20]1[CH:31]=[C:30]([O:32][CH3:33])[CH:29]=[CH:28][C:21]=1[C:22]([C:2]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])=[O:23]

Participants

4

Reactant 3

HCID 899062-Bromo-5-methoxybenzoic acidHCID 18931181HCID 18931181, compoundHCID 178418339Butyllithium

Product 1

HCID 69213029HCID 69213029, compound

Procedure

This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with 2,4-dimethoxy-N-methoxy-N-methylbenzamide. It is used in crude form in the following reaction.

Workup

  1. customThis compound is synthesized
  2. customin the following reaction

Sources & evidence

ORD record
ord-762c090ee2214ddfbc13daa68d4b1338
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Reaction notes

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