2-Bromo-5-methoxybenzoic acid → HCID 69209013, compound

HRID 30036Notes

Reaction equation

HRID 30036 reaction equation
Br[C:2]1[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].C([Li])CCC.[C:18]1([C:24]2[CH:35]=[CH:34][C:27]([C:28](N(OC)C)=[O:29])=[CH:26][CH:25]=2)[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:24]1([C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=2)[CH:25]=[CH:26][C:27]([C:28]([C:2]2[CH:10]=[CH:9][C:8]([O:11][CH3:12])=[CH:7][C:3]=2[C:4]([OH:6])=[O:5])=[O:29])=[CH:34][CH:35]=1

Participants

4

Reactant 3

HCID 899062-Bromo-5-methoxybenzoic acidHCID 10060247N-Methoxy-N-methyl-4-phenylbenzamideHCID 178418339Butyllithium

Product 1

HCID 69209013HCID 69209013, compound

Procedure

This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with 4-phenyl-N-methoxy-N-methylbenzamide.

Workup

  1. customThis compound is synthesized

Sources & evidence

ORD record
ord-818fe6e421a0494398c920fefb8450e1
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Reaction notes

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