Ammonium Chloride → HCID 86629013, compound

HRID 30185Notes

Reaction equation

[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH:9]1[CH2:14][C:15]([OH:17])=O)=[O:7])([CH3:4])([CH3:3])[CH3:2].[Cl-].[NH4+:19]>>[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH:9]1[CH2:14][C:15](=[O:17])[NH2:19])=[O:7])([CH3:4])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 25517Ammonium Chloride

HCID 50585361-Boc-2-Piperidineacetic Acid

Product 1

HCID 86629013HCID 86629013, compoundYield 46.2%

Procedure

The title compound (0.92 g) wvas prepared from 2-(RS)-carboxymethyl-piperidine-1-carboxylic acid tert butyl ester (2.0 g) and ammonium chloride (0.86 g) according to the method of Example 97.

Sources & evidence

ORD record: ord-1144f5332b1843c28d484eec61caddb4
Source dataset: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07423052B2

Reaction notes

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