HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67157985, compound → HCID 67157391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67157985 | HCID 67157985 | — |
| Reactant | HCID 178418546 | HCID 178418546 | — |
| Product | HCID 67157391 | HCID 67157391 | 13.5% |
Reaction Steps
The title compound (50 mg) was prepared by treating the compound of example 167 (0.410 g) with copper(I)cyanide (0.103 g) according to the method of example 96. Following column chromatography, further purification by HPLC was required (Supercosil ABZ+, 5-95% acetonitrile containing 0.1% trifluoroacetic acid-water containing 0.1% trifluoroacetic acid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423052B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-f7ebaa1b413047099e0c64062fb383d4 |
| Source note | uspto-grants-2008_09 |