N-bromobutanimide → HCID 67157992, compound

HRID 30195Notes

Reaction equation

HRID 30195 reaction equation
[CH3:1][C:2]1[S:3][C:4]([C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)=[C:5]([C:7]([N:9]2[CH2:14][CH2:13][CH2:12][CH2:11][CH:10]2[CH2:15][C:16]2[O:17][CH:18]=[C:19]([C:21]3[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=3)[N:20]=2)=[O:8])[N:6]=1.[Br:33]N1C(=O)CCC1=O>>[Br:33][C:18]1[O:17][C:16]([CH2:15][CH:10]2[CH2:11][CH2:12][CH2:13][CH2:14][N:9]2[C:7]([C:5]2[N:6]=[C:2]([CH3:1])[S:3][C:4]=2[C:27]2[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=2)=[O:8])=[N:20][C:19]=1[C:21]1[CH:22]=[CH:23][CH:24]=[CH:25][CH:26]=1

Participants

3

Reactant 2

HCID 67184N-bromobutanimideHCID 67158611HCID 67158611, compound

Product 1

HCID 67157992HCID 67157992, compoundYield 69.1%

Procedure

The title compound (0.075 g) was prepared by treating the compound of example 168 (0.093 g) with N-bromosuccinimide (0.037 g) according to the method of example 164.

Sources & evidence

ORD record
ord-a1dad14f4b32412e9d89be2db31a497f
Source dataset
uspto-grants-2008_09
Patent number
US07423052B2

Reaction notes

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