HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67205028, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Benzyl-3-thiophen-3-yl-piperidine-4-carboxylic acid ethyl ester | HCID 67206722 | — |
| Product | HCID 67205028 | HCID 67205028 | — |
Reaction Steps
The product from step c) (4.78 g, 14.5 mmol) was treated with 4 M HCl at 100° C. for 16 hours. Next, the reaction was evaporated to dryness, azeotroped with toluene (2×50 ml) and placed on the high vacuum to give the subtitle compound. MS calculated for C17H19NO2S−H 300, observed 300.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423056B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-4dc042578c4b4a0192d3e358b14f5c06 |
| Source note | uspto-grants-2008_09 |