HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67207170, compound → HCID 67205268, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67207170 | HCID 67207170 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 67205268 | HCID 67205268 | 100% |
Reaction Steps
The product from step b) (6.83 g, 20.7 mmol) was treated with 4 M HCl (400 ml) at 100° C. for 16 hours. Next, the reaction was evaporated to dryness, azeotroped with toluene (2×50 ml) and placed on the high vacuum to give the subtitle compound (7 g, 100%). MS calculated for C17H19NO2S−H 300, observed 300.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423056B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-e0d5c49fb9164094b73fa7fe61b9045d |
| Source note | uspto-grants-2008_09 |