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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 30278Generated: October 28, 2026

HCID 67207170, compound → HCID 67205268, compound

https://huagongshe.com/reaction/30278

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67207170HCID 67207170—
SolventHydrochloric AcidHCID 313—
ProductHCID 67205268HCID 67205268100%

Reaction Steps

The product from step b) (6.83 g, 20.7 mmol) was treated with 4 M HCl (400 ml) at 100° C. for 16 hours. Next, the reaction was evaporated to dryness, azeotroped with toluene (2×50 ml) and placed on the high vacuum to give the subtitle compound (7 g, 100%). MS calculated for C17H19NO2S−H 300, observed 300.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07423056B2
Source datasetuspto-grants-2008_09
ORD IDord-e0d5c49fb9164094b73fa7fe61b9045d
Source noteuspto-grants-2008_09