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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 30286Generated: October 29, 2026

HCID 67206463, compound → HCID 67206550, compound

https://huagongshe.com/reaction/30286

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67206463HCID 67206463—
Reactant1,2,3,3a,7,7a-Hexahydro-4-thia-2-aza-cyclopenta[alpha]pentalene-6-carbonitrileHCID 68301759—
SolventHydrochloric AcidHCID 313—
ProductHCID 67206550HCID 67206550—

Reaction Conditions

Temperature80 °C

Reaction Steps

The product from step b), diastereomer 1 (1.4 g, 4.3 mmol) was dissolved in 12 M HCl (10 mL) and was stirred at 80° C. for 12 hours. The reaction mix then was cooled to room temperature and evaporated to dryness to afford the subtitle compound. MS calculated for C17H19NO2S+H: 302, observed: 302.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07423056B2
Source datasetuspto-grants-2008_09
ORD IDord-b8dd9cd4304f498eab2284e5a0c6ae01
Source noteuspto-grants-2008_09