HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 85871665, compound → HCID 45098666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 85871665 | HCID 85871665 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 45098666 | HCID 45098666 | — |
Reaction Steps
To a solution of 1-(4-pyridyl)cyclopentanecarboxylic acid, benzyl ester (Step C, 0.36 g, 1.3 mmol) in methanol (10 mL) was added palladium on carbon (10% w/w, 75 mg). The mixture was degassed and filled with hydrogen using a balloon. After stirring overnight, the reaction mixture was filtered through Celite, and the filtrate was concentrated to dryness to afford the title compound. LC-MS: m/e 192 (M+H)+ (0.8 min).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07423067B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-f80828c4e0c14db28546774ee5327025 |
| Source note | uspto-grants-2008_09 |