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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 30393Generated: October 29, 2026

HCID 85871665, compound → HCID 45098666, compound

https://huagongshe.com/reaction/30393

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 85871665HCID 85871665—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 45098666HCID 45098666—

Reaction Steps

To a solution of 1-(4-pyridyl)cyclopentanecarboxylic acid, benzyl ester (Step C, 0.36 g, 1.3 mmol) in methanol (10 mL) was added palladium on carbon (10% w/w, 75 mg). The mixture was degassed and filled with hydrogen using a balloon. After stirring overnight, the reaction mixture was filtered through Celite, and the filtrate was concentrated to dryness to afford the title compound. LC-MS: m/e 192 (M+H)+ (0.8 min).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07423067B2
Source datasetuspto-grants-2008_09
ORD IDord-f80828c4e0c14db28546774ee5327025
Source noteuspto-grants-2008_09