HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-(3-bromopropoxy)propane → [(S)-5-(2-Ethoxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-(3-bromopropoxy)propane | HCID 11230705 | — |
| Reactant | ((S)-6-Oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl)-carbamic acid tert-butyl ester | HCID 58972520 | — |
| Product | [(S)-5-(2-Ethoxy-ethyl)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl]-carbamic acid tert-butyl ester | HCID 58972483 | — |
Reaction Steps
Using ((S)-6-oxo-6,7-dihydro-5H-dibenzo[b,d]azepin-7-yl)-carbamic acid tert-butyl ester and 2-bromomethyl-ethyl ether, the title product was prepared in the same manner as described for example 1a (83%). Pink, viscous oil. MS: m/e=397(M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425551B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-e4fc35a743ef4d149e40a0dabf7a84a9 |
| Source note | uspto-grants-2008_09 |