HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-Fluorophenyl)chroman-6-ol → 2-(3-Bromophenyl)chroman-6-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-Fluorophenyl)chroman-6-ol | HCID 17978471 | — |
| Reactant | 2-(3-Bromophenyl)chroman-4,6-diol | HCID 17978476 | — |
| Product | 2-(3-Bromophenyl)chroman-6-ol | HCID 17978598 | — |
Reaction Steps
2-(3-Bromophenyl)chroman-6-ol was prepared as described for 2-(3-fluorophenyl)chroman-6-ol in Example 9(c) starting from 700 mg of 2-(3-bromophenyl)chroman-4,6-diol. 1H NMR (400 MHz, d6-DMSO) δ: 8.81 (s, 1H), 7.61 (m, 1H), 7.51 (m, 1H), 7.43 (m, 1H), 7.35 (m, 1H), 6.67-6.48 (m, 3H), 5.01 (m, 1H), 2.87 (m, 1H), 2.63 (m, 1H), 2.12 (m, 1H), 1.92 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425568B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-4e015c321b60408098f08dbb2cd4814a |
| Source note | uspto-grants-2008_09 |