HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2-Nitrophenoxy)-2-phenylindane → 2-(2-Phenylindan-5-yloxy)phenylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2-Nitrophenoxy)-2-phenylindane | HCID 17978534 | — |
| Reactant | 2-(2-Phenylchroman-6-yloxy)-aniline | HCID 17978558 | — |
| Product | 2-(2-Phenylindan-5-yloxy)phenylamine | HCID 17978652 | — |
Reaction Steps
2-(2-Phenylindan-5-yloxy)phenylamine was prepared as described for 2-(2-phenylchroman-6yloxy)-phenylamine in Example 29(b) using 170 mg of 5-(2-nitrophenoxy)-2-phenylindane. 1H-N (400 MHz, d6-DMSO): 7.32-7.27 (m, 4H), 7.23-7.16 (m, 2H), 6.92-6.87 (m, 1H), 6.81-6.71 (m, 4H), 6.56-6.53 (m, 1H), 4.85 (bs, 2H), 3.65 (k, 1H, J 8.3 Hz), 3.23 (dd, 2H, J 8.3, 15.5 Hz), 2.97-2.88 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07425568B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-e33490f44b364434a807068d3670c16d |
| Source note | uspto-grants-2008_09 |